1-异氰酸-3,5-二甲氧基苯酯合成路线 （共 28 条）
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C 5: 28.8 g / fluoroboric acid, sodium nitrite / H2O 6: 7.6 g / warming, distillation 7: 60 percent / lithium chips / 0.5 h View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C
5: 28.8 g / fluoroboric acid, sodium nitrite / H2O
6: 7.6 g / warming, distillation
7: 1.) lithium / 1.) ether, 2 h
View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C
5: 28.8 g / fluoroboric acid, sodium nitrite / H2O
6: 7.6 g / warming, distillation
7: 1.) lithium / 1.) ether, 2 h
8: decarboxylation
View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C
5: 28.8 g / fluoroboric acid, sodium nitrite / H2O
6: 7.6 g / warming, distillation
7: 1.456 g / boron tribromide / CH2Cl2 / 52 h
View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C
5: 28.8 g / fluoroboric acid, sodium nitrite / H2O
6: 7.6 g / warming, distillation
7: 1.) lithium / 1.) ether, 2 h
8: Cu-quinoline
9: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C
View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
1: 8.7 g / sodium hydroxide (20percent) / 60 °C
5: 28.8 g / fluoroboric acid, sodium nitrite / H2O
6: 7.6 g / warming, distillation
7: 1.) lithium / 1.) ether, 2 h
8: Cu-quinoline
View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
