b-氧代-a-苯基苯丙腈合成路线 (共 38 条)
反应条件
T=700°C; flash vacuum thermolysis;
参考文献
George, Lisa; Bernhardt, Paul V.; Netsch, Klaus-Peter; Wentrup, Curt
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3518 - 3523
参考文献
Atkinson; Ingham; Thorpe
Journal of the Chemical Society, 1907 , vol. 91, p. 592
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Walther; Schickler
Journal fuer Praktische Chemie (Leipzig), 1897 , vol. <2> 55, p. 323
反应条件
sodium hydride
1.) DMF, 10 min, 2.) DMF, RT, 1 h; Yield given. Multistep reaction;
参考文献
Miyashita, Akira; Suzuki, Yumiko; Nagasaki, Izuru; Ishiguro, Chie; Iwamoto, Ken-Ichi; Higashino, Takeo
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 8 p. 1254 - 1258
参考文献
Dornow; Grabhoefer
Chemische Berichte, 1958 , vol. 91, p. 1824,1828
反应条件
in various solvent(s)
T=63.3°C; var.temperatures; ΔG(excit.), ΔH(excit.), ΔS(excit.); var. temperatures; Rate constantThermodynamic dataKinetics;
参考文献
Hassner, Alfred; Wiegand, Norbert H.; Gottlieb, Hugo E.
Journal of Organic Chemistry, 1986 , vol. 51, # 16 p. 3176 - 3180
反应条件
MeSCN; tributylphosphine; sodium hydride
1.) 0 deg C, 1 h; room temperature, 2 h, 2.) DMF, room temperature, 2 h; Yield given. Multistep reaction;
参考文献
Yokoyama, Masataka; Ohteki, Hiroko; Kurauchi, Masahiko; Hoshi, Kazuko; Yanagisawa, Eizaburo; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2635 - 2640
反应条件
in 1,2-dichloro-benzene
Heating; Mechanism;
参考文献
Belinka, Benjamin A.; Hassner, Alfred; Hendler, J. M.
Journal of Organic Chemistry, 1981 , vol. 46, # 3 p. 631 - 632
反应条件
in 1,2-dichloro-benzene
Heating; Mechanism;
参考文献
Belinka, Benjamin A.; Hassner, Alfred; Hendler, J. M.
Journal of Organic Chemistry, 1981 , vol. 46, # 3 p. 631 - 632
反应条件
in 1,2-dichloro-benzene
Heating; Mechanism;
参考文献
Belinka, Benjamin A.; Hassner, Alfred; Hendler, J. M.
Journal of Organic Chemistry, 1981 , vol. 46, # 3 p. 631 - 632
参考文献
Rupe; Gisiger
Helvetica Chimica Acta, 1925 , vol. 8, p. 349
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Bodroux
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1911 , vol. 152, p. 1594
Bulletin de la Societe Chimique de France, 1911 , vol. <4> 9, p. 726