1: SOCl2
2: BuLi / tetrahydrofuran; hexane / 8 h
3: 1 h / 700 °C / 0 - 0.05 Torr
View Scheme
参考文献
Aitken, R. Alan; Boeters, Christine; Morrison, John J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2473 - 2480
1: BuLi / tetrahydrofuran; hexane / 8 h
2: 1 h / 700 °C / 0 - 0.05 Torr
View Scheme
参考文献
Aitken, R. Alan; Boeters, Christine; Morrison, John J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2473 - 2480
T=700°C; P=0.001 - 0.05 Torr; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aitken, R. Alan; Boeters, Christine; Morrison, John J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2473 - 2480
