顺-4,7-二氢-1,3-二氧杂环庚合成路线 （共 18 条）
反应条件
dihydridotetrakis(triphenylphosphine)ruthenium(II) in neat (no solvent)
T=100°C; 1 h;
参考文献
Suzuki, Hiroharu; Yashima, Hidehiko; Hirose, Toshiyuki; Takahashi, Mitsuru; Moro-Oka, Yshihiko; Ikawa, Tsuneo
Tetrahedron Letters, 1980 , vol. 21, p. 4927 - 4930
反应条件
[rhodium(I)(carbonyl)2(acetylacetonate)]; hydrogen; 1,2-O-Isopropylidene-3,5-bis[(3,3',5,5'-tetra-tert-butyl-1,1'-biphenyl-2,2'-diyl)phosphite]-6-deoxy-β-L-talofuranose in toluene
T=45°C; P=13501.4 Torr; 4 h; Autoclave; optical yield given as percent eeenantioselective reaction;
参考文献
Mazuela, Javier; Coll, Mercedes; Pamies, Oscar; Dieguez, Montserrat
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5440 - 5445
反应条件
copper(II) sulfate
T=70°C; 0.166667 h; solvent: (iPrC6H12)3N; Yield given;
参考文献
Jendralla, Heiner
Chemische Berichte, 1982 , vol. 115, # 1 p. 201 - 209
反应条件
triethylamine in toluene
T=50°C; 48 h; Yields of byproduct given;
参考文献
Timpe, H.-J.; Schmidt, M.; Fisera, L'.
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 5 p. 735 - 747
反应条件
copper(II) sulfate
T=70°C; 0.166667 h; solvent: (iPrC6H12)3N; Yield given;
参考文献
Jendralla, Heiner
Chemische Berichte, 1982 , vol. 115, # 1 p. 201 - 209
反应条件
methanol; nickel
T=100°C; P=51485.6 Torr; Hydrogenation;
参考文献
Brannock; Lappin
Journal of Organic Chemistry, 1956 , vol. 21, p. 1366
反应条件
1: tetrachloromethane; bromine / 0 °C
2: methanol
View Scheme
参考文献
Brannock; Lappin
Journal of Organic Chemistry, 1956 , vol. 21, p. 1366
反应条件
sodium hydroxide; ethanol; N-benzyl-N,N,N-triethylammonium chloride
40 h; Ambient temperature;
参考文献
Vafina, R.M.; Kataeva, O.N.; Litvinov, I.A.; Sergeeva, G.N.; Klimovitskii, E.N.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 9.2 p. 1567 - 1572
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 9 p. 1885 - 1890
