4,7-二氢-2-异丙基-1,3-二氧杂卓合成路线 （共 8 条）
参考文献
Takeda Chemical Industries, Ltd.
Patent: US4339586 A1, 1982 ;
反应条件
T=90 - 155°C; Diels-Alder Reaction; P=112.511 - 760.051 Torr; 4 - 24 h; Product distribution / selectivity;
参考文献
DSM IP ASSETS B.V.
Patent: WO2005/49618 A1, 2005 ;
Location in patent: Page/Page column 12-14 ;
反应条件
T=90 - 155°C; Diels-Alder Reaction; P=112.511 - 760.051 Torr; 4 - 24 h; Product distribution / selectivity;
参考文献
DSM IP ASSETS B.V.
Patent: WO2005/49618 A1, 2005 ;
Location in patent: Page/Page column 12-14 ;
参考文献
L'vova,S.D. et al.
Pharmaceutical Chemistry Journal, 1978 , vol. 12, # 12 p. 1636 - 1638
Khimiko-Farmatsevticheskii Zhurnal, 1978 , vol. 12, # 12 p. 106 - 109
反应条件
toluene-4-sulfonic acid in hexane
Heating;
参考文献
Hilf, Stefan; Berger-Nicoletti, Elena; Grubbs, Robert H.; Kilbinger, Andreas F. M.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 47 p. 8045 - 8048
反应条件
toluene-4-sulfonic acid
P=15 Torr; 24 h; Ambient temperature;
参考文献
Frauenrath, Herbert; Runsink, Jan
Journal of Organic Chemistry, 1987 , vol. 52, # 13 p. 2707 - 2712
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Abuzov, B. A.; Klimovitskii, E. N.; Remizov, A. B.; Timirbaev, M. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 5 p. 794 - 799
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 5 p. 1030 - 1036
反应条件
toluene-4-sulfonic acid; benzene
参考文献
Brannock; Lappin
Journal of Organic Chemistry, 1956 , vol. 21, p. 1366
