1-(二甲基胺甲基)萘酚合成路线 （共 32 条）
反应条件
sodium cyanide; ethanol T=150°C;
参考文献
Winthrop Chem. Co.
Patent: US2315661 , 1940 ;
反应条件
in benzene 48 h; Ambient temperature;
参考文献
Blade-Font, Artur; Rocabayera, Teodoro de Mas
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 841 - 848
反应条件
methyl iodide in benzene 48 h; Ambient temperature;
参考文献
Blade-Font, Artur; Rocabayera, Teodoro de Mas
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 841 - 848
反应条件
1: 0.5 g / 0.5 h / 260 - 280 °C 2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C View Scheme
参考文献
Rosario, Christopher A.; Holder, Gerald M.; Duke, Colin C.
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1064 - 1072
反应条件
potassium carbonate in dichloromethane
0.5 h; Ambient temperature;
参考文献
Anwar, Hany F.; Skattebol, Lars; Hansen, Trond Vidar
Tetrahedron, 2007 , vol. 63, # 40 p. 9997 - 10002
反应条件
in glycerol
T=40°C; Betti Reaction; 0.0833333 h;
参考文献
Ganesan, Subramaniapillai Selva; Rajendran, Narendran; Sundarakumar, Sankahr Ilathur; Ganesan, Asaithampi; Pemiah, Brindha
Synthesis (Germany), 2013 , vol. 45, # 11 art. no. SS-2013-Z0059-OP, p. 1564 - 1568
反应条件
bis(acetylacetonate)oxovanadium in dichloromethane
24 h; Heating;
参考文献
Hwang, Der-Ren; Uang, Biing-Jiun
Organic Letters, 2002 , vol. 4, # 3 p. 463 - 466
反应条件
hydrogen tetrachloroaurate(III) trihydrate; trichloromonobromomethane in dichloromethane
T=20°C;
参考文献
Sun, Wenbo; Lin, Huacan; Zhou, Wenyu; Li, Zigang
RSC Advances, 2014 , vol. 4, # 15 p. 7491 - 7494
反应条件
hydrogen tetrachloroaurate(III) trihydrate; trichloromonobromomethane in dichloromethane
T=20°C; Inert atmosphere; Overall yield = 78 percent;
参考文献
Sun, Wenbo; Lin, Huacan; Zhou, Wenyu; Li, Zigang
RSC Advances, 2014 , vol. 4, # 15 p. 7491 - 7494
参考文献
Kreutzkamp,N.; Oei,H.-J.
Chemische Berichte, 1968 , vol. 101, # 7 p. 2459 - 2463
