反应条件
hydrogenchloride; n-butyllithium in diethyl ether; hexane (N2); addn. of a soln. of BuLi in hexane to a soln. of acetal in ether at -75°C, stirring for 1 h, addn. of boron compd., stirring at room temp. for 2.5 h, addn. of aq. HCl, refluxing for 1.5 h with stirring; sepn. of ppt., extn. with aq. NaOH, acidification of the ext.;
参考文献
Kumar, Subodh
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 9 p. 1018 - 1023
