反应条件
1: 5-bromo-1,2,3-trifluorobenzene With magnesium in diethyl ether Grignard reaction; 2: tri-isopropoxy-borane in diethyl ether T=-30 - 10°C; boronation; 0.5 h; 3: With hydrogenchloride in diethyl ether T=20°C; Hydrolysis; 1 h; Title compound not separated from byproducts;
参考文献
Frohn; Franke; Fritzen; Bardin
Journal of Organometallic Chemistry, 2000 , vol. 598, # 1 p. 127 - 135