反应条件
1: 2-(1,3-dioxolan-2-yl)ethylMgBr With ferrous acetate; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride in tetrahydrofuran
T=50 - 60°C; Kumada Cross-Coupling; 0.333333 h; Schlenk techniqueInert atmosphere;
2: 1-iodo-butane in tetrahydrofuran
T=20°C; Kumada Cross-Coupling; 8 h; Schlenk techniqueInert atmosphere;
参考文献
Guisan-Ceinos, Manuel; Tato, Francisco; Bunuel, Elena; Calle, Paloma; Cardenas, Diego J.
Chemical Science, 2013 , vol. 4, # 3 p. 1098 - 1104