反应条件
tetrabutylammomium bromide; tetra-n-butylammonium tetrafluoroborate in tetrahydrofuran
Electrochem. Process; steel anode (100 cm**2, 2.5 mA/cm**2, 40°C, 25 mF passing); solvent removing in vacuum, residue treating with hexane, resulting soln. filtration off, filtrate reduction in vacuum, residue subjecting to column chromy. (silica gel/hexane);
参考文献
Shirokii; Knizhnikov; Vinokurov; Murashko; Maier
Russian Journal of General Chemistry, 1998 , vol. 68, # 1 p. 83 - 86
