1-甲基-5-氨基四氮唑合成路线 (共 24 条)
参考文献
Murphy; Picard
Journal of Organic Chemistry, 1954 , vol. 19, p. 1807,1813
反应条件
1: in toluene
0.75 h; Heating / reflux;
2: With sodium tetrahydroborate in ethanol
T=20°C; 4 h;
3: With water; ammonium chloride in ethanol
参考文献
NOVARTIS AG
Patent: WO2008/58967 A1, 2008 ;
Location in patent: Page/Page column 44 ;
反应条件
hydrogenchloride; sodium nitrite in water
参考文献
Klapoetke, Thomas M.; Sabate, Carles Miro; Stierstorfer, Joerg
New Journal of Chemistry, 2009 , vol. 33, # 1 p. 136 - 147
参考文献
Stolle et al.
Journal fuer Praktische Chemie (Leipzig), 1932 , vol. <2>134, p. 282,297