3-氨基-1,2,4-苯并噻嗪-1-n-氧化物合成路线 (共 25 条)
反应条件
1: With hydrogenchloride T=100°C; 1 h; 2: With sodium hydroxide T=100°C; 2 h; Further stages.;
参考文献
Auckland Uniservices Limited
Patent: EP1468688 A2, 2004 ;
Location in patent: Page/Page column 23; 51 ;
反应条件
3-chloro-benzenecarboperoxoic acid in methanol; dichloromethane T=20°C; 3 h;
参考文献
EP1468688 A2, ;
Page/Page column 37; 74 ;
反应条件
3-chloro-benzenecarboperoxoic acid in methanol; dichloromethane T=20°C; 3 h;
参考文献
Magnetic Resonance in Chemistry, , vol. 44, # 10 p. 948 - 954
参考文献
Chemische Berichte, , vol. 46, p. 3529
反应条件
dihydrogen peroxide in acetic acid T=50°C; 2 h;
参考文献
Fuchs; Chowdhury; Barnes; Gates
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 107 - 114
反应条件
MeC(O)OOBu-t in water T=105 - 112°C;
参考文献
Fuchs; Chowdhury; Barnes; Gates
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 107 - 114
反应条件
sodium salt of phosphorous acid in acetonitrile 5.5 h; Ambient temperatureIrradiation;
参考文献
Daniels, J. Scott; Chatterji, Tonika; MacGillivray, Leonard R.; Gates, Kent S.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 10027 - 10030
反应条件
1: H2O2 / acetic acid / 2 h / 50 °C 2: tert-butyl peracetate / H2O / 105 - 112 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 1 p. 107 - 114
反应条件
azo-tert-butyl in 1,4-dioxane Heating;
参考文献
Shi, Xiaofeng; Poole, James S.; Emenike, Ijeoma; Burdzinski, Gotard; Platz, Matthew S.
Journal of Physical Chemistry A, 2005 , vol. 109, # 8 p. 1491 - 1496
反应条件
potassium tert-butylate 1.) THF, 60 deg C, 4 h, 2.) THF, 2 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 8 p. 855 - 857