3-氨基-1,2,4-苯并噻嗪-1-n-氧化物合成路线 （共 25 条）
反应条件
potassium tert-butylate 1.) THF, 60 deg C, 4 h, 2.) THF, 2 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 8 p. 855 - 857
参考文献
Journal of the Chemical Society, , p. 3186,3191
反应条件
1: N,N-dimethyl-aniline; POCl3 2: ethanol; NH3 View Scheme
参考文献
Journal of the Chemical Society, , p. 3186,3191
反应条件
1: durch Zusammenschmelzen und Behandeln des Reaktionsproduktes mit ueberschuessiger konz. Salzsaeure 2: diluted NaOH-solution View Scheme
参考文献
Chemische Berichte, , vol. 46, p. 3529
反应条件
water-d2 in phosphate buffer pH=7.0; 0.333333 h; Photolysisanaerobic; Product distribution;
参考文献
Chemical Research in Toxicology, , vol. 11, # 11 p. 1254 - 1257
反应条件
sulfuric acid; water; nitric acid
参考文献
Robbins; Schofield
Journal of the Chemical Society, 1957 , p. 3186,3191
反应条件
dihydrogen peroxide in acetic acid T=60 - 70°C; 10 h;
参考文献
Suzuki, Hitomi; Kawakami, Takehiko
Synthesis, 1997 , # 8 p. 855 - 857
反应条件
HOF*CH3CN in dichloromethane T=20°C;
参考文献
Gatenyo, Julia; Johnson, Kevin; Rajapakse, Anuruddha; Gates, Kent S.; Rozen, Shlomo
Tetrahedron, 2012 , vol. 68, # 43 p. 8942 - 8944
反应条件
sodium dithionite in ethanol
1 h; Heating;
参考文献
Gauthier; Duceppe
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 4 p. 1081 - 1086
反应条件
1: 80 percent / NaNO2; TFA / ethyl acetate / 2 Torr
2: 92 percent / POCl3 / dimethylformamide / 1 h / Heating
3: 33 percent / H2 / Pd/C / ethanol; ethyl acetate / 2 h / 3102.97 Torr
View Scheme
参考文献
Boyd, Maruta; Hay, Michael P.; Boyd, Peter D. W.
Magnetic Resonance in Chemistry, 2006 , vol. 44, # 10 p. 948 - 954
