2,4-二氯-6-甲基嘧啶合成路线 (共 66 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; water; toluene
Suzuki Coupling; 48 h; HeatingInert atmosphere;
参考文献
Achelle, Sylvain; Robin-Le Guen, Francoise
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4491 - 4496
反应条件
in tetrahydrofuran
T=20°C;
参考文献
Baumann, Karlheinz; Flohr, Alexander; Goetschi, Erwin; Jacobsen, Helmut; Jolidon, Synese; Luebbers, Thomas
Patent: US2009/215759 A1, 2009 ;
Location in patent: Page/Page column 48 ;
反应条件
188 h; Heatingother reaction time (8, 16, 24, 48, and 72 hours); Product distribution;
参考文献
Gershon; Grefig; Clarke
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 1 p. 205 - 209
反应条件
1: acetic acid
View Scheme
参考文献
Endicott; Johnson
Journal of the American Chemical Society, 1941 , vol. 63, p. 1286,1288
参考文献
Chi; Ling
Scientia Sinica (English Edition), 1955 , vol. 4, p. 119,125
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Andrisano
Bollettino Scientifico della Facolta di Chimica Industriale di Bologna, 1944 , vol. 5, p. 48,51
参考文献
Garner, James; Hill, Tim; Odell, Luke; Keller, Paul; Morgan, Jody; McCluskey, Adam
Australian Journal of Chemistry, 2004 , vol. 57, # 11 p. 1079 - 1083