3-苯基-3-苯基硫基丙酸合成路线 （共 13 条）
反应条件
1: SOCl2 / benzene / Heating 2: HCl / diethyl ether; CHCl3 3: AcOH View Scheme
参考文献
Rosnati,V. et al.
Gazzetta Chimica Italiana, 1976 , vol. 106, p. 641 - 649
反应条件
tetrabutyl ammonium fluoride
T=50°C; 24 h;
参考文献
Gao, Shijay; Tseng, Chi; Tsai, Cheng Hsuan; Yao, Ching-Fa
Tetrahedron, 2008 , vol. 64, # 8 p. 1955 - 1961
参考文献
Zahouily, Mohamed; Mounir, Bahija; Cherki, Hind; Bahlaouan, Bouchaib; Rayadh, Ahmed; Sebti, Said
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 6 p. 1203 - 1217
反应条件
in diethyl ether
16 h; under nitrogen; Title compound not separated from byproducts;
参考文献
Detty, Michael R.; Wood, Gary P.
Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 80 - 89
反应条件
1: 80 percent / thionyl chloride / diethyl ether
2: 79 percent / H2SO4
3: 91 percent / NaOH
View Scheme
参考文献
Zahouily, Mohamed; Mounir, Bahija; Cherki, Hind; Bahlaouan, Bouchaib; Rayadh, Ahmed; Sebti, Said
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 6 p. 1203 - 1217
反应条件
1: H2NOH*HCl; lithium nitrate/natural phosphate
2: 80 percent / thionyl chloride / diethyl ether
3: 79 percent / H2SO4
4: 91 percent / NaOH
View Scheme
参考文献
Zahouily, Mohamed; Mounir, Bahija; Cherki, Hind; Bahlaouan, Bouchaib; Rayadh, Ahmed; Sebti, Said
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 6 p. 1203 - 1217
反应条件
1: 95 percent / natural phosphate / methanol / 15 h / 20 °C
2: H2NOH*HCl; lithium nitrate/natural phosphate
3: 80 percent / thionyl chloride / diethyl ether
4: 79 percent / H2SO4
5: 91 percent / NaOH
View Scheme
参考文献
Zahouily, Mohamed; Mounir, Bahija; Cherki, Hind; Bahlaouan, Bouchaib; Rayadh, Ahmed; Sebti, Said
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 6 p. 1203 - 1217
反应条件
1: 95 percent / natural phosphate / methanol / 15 h / 20 °C
2: H2NOH*HCl; lithium nitrate/natural phosphate
3: 80 percent / thionyl chloride / diethyl ether
4: 79 percent / H2SO4
5: 91 percent / NaOH
View Scheme
参考文献
Zahouily, Mohamed; Mounir, Bahija; Cherki, Hind; Bahlaouan, Bouchaib; Rayadh, Ahmed; Sebti, Said
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 6 p. 1203 - 1217
反应条件
hydrogen bromide; acetic acid
T=100°C; im Rohr;
参考文献
Arndt
Chemische Berichte, 1923 , vol. 56, p. 1275
Chemische Berichte, 1925 , vol. 58, p. 1632
反应条件
1: 79 percent / H2SO4
2: 91 percent / NaOH
View Scheme
参考文献
Zahouily, Mohamed; Mounir, Bahija; Cherki, Hind; Bahlaouan, Bouchaib; Rayadh, Ahmed; Sebti, Said
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 6 p. 1203 - 1217
