6,7-二氢-5H-苯并[c]咔唑合成路线 （共 9 条）
反应条件
chloranil in xylene 2 h; Inert atmosphereReflux;
参考文献
LG Chem, Ltd.
Patent: EP2332911 A2, 2011 ;
Location in patent: Page/Page column 59; 60 ;
反应条件
acetic acid in ethanol
2 h; RefluxInert atmosphere;
参考文献
LG Chem, Ltd.
Patent: EP2332911 A2, 2011 ;
Location in patent: Page/Page column 59; 60 ;
反应条件
[Au(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)(bis-(trifluoromethanesulfonyl)imidate)] in 1,2-dichloro-ethane
T=80°C; 3 h;
参考文献
Lu, Biao; Luo, Yingdong; Liu, Lianzhu; Ye, Longwu; Wang, Yanzhao; Zhang, Liming
Angewandte Chemie - International Edition, 2011 , vol. 50, # 36 p. 8358 - 8362
反应条件
hydrogenchloride in water
T=100°C; 6 h;
参考文献
Katrizky, Alan R.; Wang, Zuoquan
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 2 p. 671 - 675
参考文献
Ghigi
Gazzetta Chimica Italiana, 1930 , vol. 60, p. 194,198
Gazzetta Chimica Italiana, 1931 , vol. 61, p. 43,46
反应条件
potassium tert-butylate in ammonia
2 h; Photolysis;
参考文献
Barolo, Silvia M.; Lukach, Andres E.; Rossi, Roberto A.
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2807 - 2811
参考文献
Ghigi
Gazzetta Chimica Italiana, 1930 , vol. 60, p. 194,198
Gazzetta Chimica Italiana, 1931 , vol. 61, p. 43,46
参考文献
Ghigi
Gazzetta Chimica Italiana, 1931 , vol. 61, p. 43,45, 46
反应条件
1: chloranil / xylene / 2 h / Inert atmosphere; Reflux
2: sodium t-butanolate / Pd0(tris(tert-butyl)phosphine)2 / xylene / 7 h / Reflux; Inert atmosphere
View Scheme
参考文献
LG Chem, Ltd.
Patent: EP2332911 A2, 2011 ;
