C-(3,4-二氢-2H-苯并[1,4]嗪-3-基)-甲胺合成路线 （共 5 条）
反应条件
1: 81 percent / H2 / Pd-C / ethanol / 24 h
2: hydrazine hydrate / ethanol / 3 h / Heating
View Scheme
参考文献
Romeo, Giuseppe; Materia, Luisa; Manetti, Fabrizio; Cagnotto, Alfredo; Mennini, Tiziana; Nicoletti, Ferdinando; Botta, Maurizio; Russo, Filippo; Minneman, Kenneth P.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 14 p. 2877 - 2894
反应条件
sodium hydroxide in ethanol
28 h; Heating;
参考文献
Gupta,S.P. et al.
Indian Journal of Chemistry, 1975 , vol. 13, p. 462 - 467
反应条件
1: 87 percent / Dess-Martin periodinane / CH2Cl2; dimethylsulfoxide / 3 h / 60 °C
2: 81 percent / H2 / Pd-C / ethanol / 24 h
3: hydrazine hydrate / ethanol / 3 h / Heating
View Scheme
参考文献
Romeo, Giuseppe; Materia, Luisa; Manetti, Fabrizio; Cagnotto, Alfredo; Mennini, Tiziana; Nicoletti, Ferdinando; Botta, Maurizio; Russo, Filippo; Minneman, Kenneth P.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 14 p. 2877 - 2894
反应条件
hydrazine hydrate in ethanol
3 h; Heating;
参考文献
Gupta,S.P. et al.
Indian Journal of Chemistry, 1975 , vol. 13, p. 462 - 467
反应条件
1: H2 / Raney-Ni / ethanol
2: aq. NaOH / ethanol / 28 h / Heating
View Scheme
参考文献
Gupta,S.P. et al.
Indian Journal of Chemistry, 1975 , vol. 13, p. 462 - 467
