6-溴-2-甲基喹唑啉-4-酮合成路线 （共 7 条）
反应条件
1: 2-amino-5-bromo-benzoic acid With ammonia 1 h; Heating / reflux; 2: acetic anhydride 4 h; Heating / reflux; 3: With water 0.5 h; Heating / reflux;
参考文献
Gruenenthal GmbH
Patent: US2009/69320 A1, 2009 ;
Location in patent: Page/Page column 76 ;
反应条件
urea-hydrogen peroxide; potassium carbonate in water; acetone 2 h; Heating;
参考文献
Bandgar
Synthetic Communications, 1997 , vol. 27, # 12 p. 2065 - 2068
反应条件
1: in N,N-dimethyl-formamide T=20°C; 0.166667 h; Inert atmosphere; 2: With iron (III) acetylacetonate; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide Microwave irradiationInert atmosphere;
参考文献
Zhang, Xiaodong; Ye, Deju; Sun, Haifeng; Guo, Diliang; Wang, Jiang; Huang, He; Zhang, Xu; Jiang, Hualiang; Liu, Hong
Green Chemistry, 2009 , vol. 11, # 11 p. 1881 - 1888
反应条件
ammonium acetate T=170 - 180°C; 0.0833333 h;
参考文献
Journal of Chemical & Engineering Data, , vol. 26, # 1 p. 103 - 104
参考文献
Journal of the American Chemical Society, , vol. 28, p. 101
反应条件
1: 2 h / Heating 2: ammonium acetate / 0.08 h / 170 - 180 °C View Scheme
参考文献
Journal of Chemical & Engineering Data, , vol. 26, # 1 p. 103 - 104
参考文献
Proceedings - Indian Academy of Sciences, Section A, , vol. 13, p. 50
Chem.Abstr., , p. 5502
