4,7-二溴-2,1,3-苯噁二唑合成路线 （共 12 条）
反应条件
bromine; iron T=90°C; 3 h; Reflux;
参考文献
Coombs, Benjamin A.; Lindner, Benjamin D.; Edkins, Robert M.; Rominger, Frank; Beeby, Andrew; Bunz, Uwe H. F.
New Journal of Chemistry, 2012 , vol. 36, # 3 p. 550 - 553
反应条件
bromine; iron in dichloromethane T=100°C; 1 h;
参考文献
Onoda, Maki; Tokuyama, Hidetoshi; Uchiyama, Seiichi; Mawatari, Ken-Ichi; Santa, Tomofumi; Kaneko, Kiyoko; Imai, Kazuhiro; Nakagomi, Kazuya
Chemical Communications, 2005 , # 14 p. 1848 - 1850
反应条件
hydrogenchloride; potassium hydroxide; hydroxylamine
参考文献
Journal of the Chemical Society, , p. 3308
反应条件
1: toluene / Heating 2: NH2OH*HCl, aq. KOH / ethanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 29, p. 3722 - 3723
反应条件
1: NH3 / ethanol 2: (i) NaNO2, H2SO4, AcOH, (ii) aq. NaN3 3: toluene / Heating 4: NH2OH*HCl, aq. KOH / ethanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 29, p. 3722 - 3723
反应条件
1: bromine; CS2 2: aq.-ethanolic KOH 3: NH2OH+HCl; aq.-ethanolic KOH View Scheme
参考文献
Journal of the Chemical Society, , p. 3308
反应条件
1: sodium hypochlorite; tetrabutylammomium bromide; sodium hydroxide / diethyl ether / 20 °C 2: morpholine; sulfur / ethylene glycol / 150 °C 3: bromine; iron / 90 °C View Scheme
参考文献
Dyes and Pigments, , vol. 95, # 2 p. 229 - 235
反应条件
1.1: silica gel; sulfuric acid / |Inert atmosphere 1.2: |Inert atmosphere 2.1: toluene / |Heating; |Inert atmosphere 3.1: triethyl phosphite / ethanol / |Reflux; |Inert atmosphere 4.1: iron / |Inert atmosphere View Scheme
参考文献
Journal of Polymer Science, Part A: Polymer Chemistry, , vol. 50, # 19 p. 3996 - 4003
反应条件
1: toluene / |Heating; |Inert atmosphere 2: triethyl phosphite / ethanol / |Reflux; |Inert atmosphere 3: iron / |Inert atmosphere View Scheme
参考文献
Journal of Polymer Science, Part A: Polymer Chemistry, , vol. 50, # 19 p. 3996 - 4003
参考文献
Journal of the Chemical Society, , p. 3308
