1,1,6,6-四甲氧基己烷合成路线 (共 5 条)
反应条件
sulfuric acid in methanol
3 h; Ambient temperature;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kashimura, Shigenori
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3338 - 3340
反应条件
1: 77 percent / tetraethylammonium p-toluenesulfonate / electrolysis (6 F/mol, 0.5 A)
2: 74 percent / 5percent H2SO4 / methanol / 3 h / Ambient temperature
View Scheme
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kashimura, Shigenori
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3338 - 3340
反应条件
2,3-dimercapto-succinic acid; ozone
1) -50 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Griesbaum, Karl; Jung, In Chang; Mertens, Henri
Journal of Organic Chemistry, 1990 , vol. 55, # 24 p. 6024 - 6027
反应条件
sulfuric acid; oxygen
Irradiation;
参考文献
Treibs,W.; Schoellner,R.
Chemische Berichte, 1961 , vol. 94, p. 2983 - 2989
反应条件
hydrogenchloride; ozone
-78 deg to r.t.; Product distribution;
参考文献
Griesbaum, Karl; Neumeister, Joachim
Chemische Berichte, 1982 , vol. 115, # 8 p. 2697 - 2706