4-(4-甲氧基亚苄基)-2-苯基-2-噁唑烷-5-酮合成路线 (共 27 条)
反应条件
ammonium acetate in acetic acid Heating;
参考文献
Bansal, R. K.; Jain, Jainendra K.
Synthesis, 1986 , # 10 p. 840 - 842
反应条件
in benzene 3 h; Heating; Yield given. Title compound not separated from byproducts;
参考文献
Gelmi, M. Luisa; Pocar, Donato; Viziano, Monica; Destro, Riccardo; Merati, Felicita
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 6 p. 701 - 706
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone 1.) anisole, reflux, 6 h, 2.) reflux, 1 h; Yield given. Multistep reaction;
参考文献
Gelmi, M. Luisa; Pocar, Donato; Viziano, Monica; Destro, Riccardo; Merati, Felicita
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 6 p. 701 - 706
反应条件
1: aq. HNO3 / -25 - 0 °C View Scheme
参考文献
Walter,R.; Zimmer,H.
Journal fuer Praktische Chemie (Leipzig), 1964 , vol. 26, p. 127 - 129
反应条件
sodium hydroxide in water 0.5 h;
参考文献
Baranov, Mikhail S.; Lukyanov, Konstantin A.; Ivashkin, Pavel E.; Yampolsky, Ilia V.
Synthetic Communications, 2013 , vol. 43, # 17 p. 2337 - 2342
反应条件
acetic acid T=120°C; 0.25 h; Microwave irradiation;
参考文献
Wang, Shu-Liang; Ding, Jie; Jiang, Bo; Gao, Yuan; Tu, Shu-Jiang
ACS Combinatorial Science, 2011 , vol. 13, # 5 p. 572 - 577
反应条件
trifluoroacetic acid in N,N-dimethyl-formamide 0.25 h; Microwave irradiation;
参考文献
Wang, Shu-Liang; Ding, Jie; Jiang, Bo; Gao, Yuan; Tu, Shu-Jiang
ACS Combinatorial Science, 2011 , vol. 13, # 5 p. 572 - 577
反应条件
1.1: sodium hydroxide / 6 h / Heating 1.2: H2O2; sodium hydroxide / H2O / cooling 2.1: HCl View Scheme
参考文献
Mahajan; Pikle
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 6 p. 1554 - 1556
反应条件
man saeuert mit Eisessig an und oxydiert mit Wasserstoffperoxyd-Loesung;
参考文献
Mauthner
Justus Liebigs Annalen der Chemie, 1909 , vol. 370, p. 374
反应条件
samarium; acetic anhydride
0.0666667 h; Microwave irradiation;
参考文献
Ahmadi, Seyed Javad; Sadjadi, Sodeh; Hosseinpour, Morteza
Ultrasonics Sonochemistry, 2013 , vol. 20, # 1 p. 408 - 412