1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0.5 h / 0 - 5 °C
2: magnesium / methanol / 20 °C
View Scheme
参考文献
Kumar, Padam Praveen; Reddy, Y. Dathu; Kumari, Y. Bharathi; Devi, B. Rama; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 4 p. 392 - 398
1: thionyl chloride / 0.25 h / 0 - 5 °C
2: magnesium / methanol / 20 °C
View Scheme
参考文献
Kumar, Padam Praveen; Reddy, Y. Dathu; Kumari, Y. Bharathi; Devi, B. Rama; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 4 p. 392 - 398
potassium hexamethylsilazane
multistep reaction, anionic <3,3>-sigmatropic rearrangement of N-phenyl-O-acylhydroxylamines, other N-phenyl-N-acetyl-O-acylhydroxylamines as educts; Product distribution;
