5-氯-4-羟基-2H-色烯-2-酮合成路线 （共 2 条）
反应条件
1: 1) BuLi, 2) ZnCl2, 3) PdCl2(PPh3)2, DIBAL-H / 1) THF, -78 deg C, 2) THF, -78 deg C, 3) THF, 0 deg C to RT
2: 84 percent / NaH / tetrahydrofuran / Heating
3: 82 percent / TFA / toluene / 1 h / Heating
View Scheme
参考文献
Kalinin, Alexey V.; Da Silva, Alcides J. M.; Lopes, Claudio C.; Lopes, Rosangela S. C.; Snieckus, Victor
Tetrahedron Letters, 1998 , vol. 39, # 28 p. 4995 - 4998
反应条件
1: 84 percent / NaH / tetrahydrofuran / Heating
2: 82 percent / TFA / toluene / 1 h / Heating
View Scheme
参考文献
Kalinin, Alexey V.; Da Silva, Alcides J. M.; Lopes, Claudio C.; Lopes, Rosangela S. C.; Snieckus, Victor
Tetrahedron Letters, 1998 , vol. 39, # 28 p. 4995 - 4998
