4-(4-二甲基氨基苯基)-3-丁烯-2-酮合成路线 （共 9 条）
反应条件
sodium hydroxide 72 h; Ambient temperature;
参考文献
Kesten, Stephen J.; Degnan, Margaret J.; Hung, Jocelyn; McNamara, Dennis J.; Ortwine, Daniel F.; et al.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 19 p. 3429 - 3447
反应条件
in chloroform; water; acetone
反应条件
1: 71 percent / Bu4NI / 1) 25 deg C, 16h, 2) 60 deg C, 2h 2: LiN(iPr)2 / tetrahydrofuran; hexane / 2 h / -78 °C 3: tetrahydrofuran; hexane / -78 °C 4: 61 percent / at standing on air View Scheme
参考文献
Chemische Berichte, , vol. 119, # 6 p. 1772 - 1800
反应条件
1: LiN(iPr)2 / tetrahydrofuran; hexane / 2 h / -78 °C 2: tetrahydrofuran; hexane / -78 °C 3: 61 percent / at standing on air View Scheme
参考文献
Chemische Berichte, , vol. 119, # 6 p. 1772 - 1800
参考文献
Huenig, Siegfried; Reichelt, Helmut
Chemische Berichte, 1986 , vol. 119, # 6 p. 1772 - 1800
反应条件
1: tetrahydrofuran; hexane / -78 °C 2: 61 percent / at standing on air View Scheme
参考文献
Chemische Berichte, , vol. 119, # 6 p. 1772 - 1800
参考文献
Chemische Berichte, , vol. 35, p. 3577
反应条件
C15H17N3F6S in ethyl acetate T=20°C; Michael addition; 120 h;
参考文献
Mei, Kul; Jin, Mel; Zhang, Shilei; Li, Ping; Liu, Wenjing; Chen, Xiaobei; Xue, Fei; Duan, Wenhu; Wang, Wei
Organic Letters, 2009 , vol. 11, # 13 p. 2864 - 2867
反应条件
sodium hydroxide; ethanol
参考文献
Rupe; Siebel
Chem. Zentralbl., 1906 , vol. 77, # II p. 1325
