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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
54357-08-3
合成路线
（共 10 条）
1345037-48-0
→
反应条件
54357-08-3
反应条件
tris-(dibenzylideneacetone)dipalladium(0); t-Bu Brett Phos; TDA; sodium nitrite in tert-butyl alcohol T=130°C; Schlenk techniqueInert atmosphere;
参考文献
De, Chandra Kanta; Pesciaioli, Fabio; List, Benjamin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 35 p. 9293 - 9295
Angew. Chem., 2013 , vol. 125, # 35 p. 9463 - 9465,3
869624-51-1
→
反应条件
54357-08-3
反应条件
in xylene 90 h; Heating;
参考文献
Bianchi, Lara; Dell'Erba, Carlo; Maccagno, Massimo; Petrillo, Giovanni; Rizzato, Egon; Sancassan, Fernando; Severi, Elda; Tavani, Cinzia
Journal of Organic Chemistry, 2005 , vol. 70, # 22 p. 8734 - 8738
90-12-0
1-甲基萘
→
反应条件
54357-08-3
反应条件
1: 6 percent Chromat. / nitric acid, acetic anhydride / -10 °C 2: 8 percent Chromat. / nitric acid, acetic anhydride / 25 °C / further reagent dinitrogen tetroxide View Scheme
参考文献
Eberson, Lennart; Radner, Finn
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 1 p. 71 - 78
91-57-6
2-甲基萘
→
反应条件
54357-08-3
反应条件
1: tetrabutylammonium hexafluorophosphate / CH2Cl2 / -70 °C / anodic oxidation 2: nitrogen dioxide / CH2Cl2 / -70 deg C -> 0 deg C View Scheme
参考文献
Eberson, Lennart; Radner, Finn
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 1 p. 71 - 78
17579-79-2
6-甲基萘-2-醇
→
反应条件
54357-08-3
反应条件
1: triethylamine / dichloromethane / 0 - 20 °C 2: tris-(dibenzylideneacetone)dipalladium(0); t-Bu Brett Phos; sodium nitrite; TDA / tert-butyl alcohol / 130 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
De, Chandra Kanta; Pesciaioli, Fabio; List, Benjamin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 35 p. 9293 - 9295
Angew. Chem., 2013 , vol. 125, # 35 p. 9463 - 9465,3
91-57-6
2-甲基萘
→
反应条件
54755-20-3
6-甲基-1-硝基萘
+
54357-08-3
+
881-03-8
2-甲基-二硝基萘酚
+
13615-38-8
3-甲基-1-硝基萘
反应条件
nitric acid; acetic anhydride T=25°C; further reagent dinitrogen tetroxide; Further byproducts given;
参考文献
Eberson, Lennart; Radner, Finn
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 1 p. 71 - 78
860746-36-7
→
反应条件
54357-08-3
反应条件
1: acetic acid; nitric acid 2: aqueous sulfuric acid 3: Diazotization.Eintragen der Diazoniumsalz-Loesung in siedendes Aethanol View Scheme
参考文献
Vesely; Pac
Collection of Czechoslovak Chemical Communications, 1930 , vol. 2, p. 471,478
860746-28-7
→
反应条件
54357-08-3
反应条件
1: aqueous sulfuric acid 2: Diazotization.Eintragen der Diazoniumsalz-Loesung in siedendes Aethanol View Scheme
参考文献
Vesely; Pac
Collection of Czechoslovak Chemical Communications, 1930 , vol. 2, p. 471,478
856212-42-5
→
反应条件
54357-08-3
反应条件
Diazotization.Eintragen der Diazoniumsalz-Loesung in siedendes Aethanol;
参考文献
Vesely; Pac
Collection of Czechoslovak Chemical Communications, 1930 , vol. 2, p. 471,478
54357-08-3
→
反应条件
17579-79-2
6-甲基萘-2-醇
反应条件
1: alcoholic ammonium hydrosulfide 2: Diazotization View Scheme
参考文献
Vesely; Kapp
Recueil des Travaux Chimiques des Pays-Bas, 1925 , vol. 44, p. 369
Chemicke Listy, vol. 18, p. 246
Chem. Zentralbl., 1924 , vol. 95, # II p. 2751
