4,4-二甲氧基-2-丁酮合成路线 (共 125 条)
参考文献
Allen et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 787,792
反应条件
toluene-4-sulfonic acid in methanol
T=20°C; 24 h;
参考文献
Bonacorso, Helio G.; Porte, Liliane M.F.; Cechinel, Cleber A.; Paim, Gisele R.; Deon, Everton D.; Zanatta, Nilo; Martins, Marcos A.P.
Tetrahedron Letters, 2009 , vol. 50, # 13 p. 1392 - 1394
反应条件
pyridinium tribromide in methanol
参考文献
Ichihara,A. et al.
Bulletin of the Chemical Society of Japan, 1965 , vol. 38, p. 1158 - 1161
反应条件
trifluoroacetic acid in tetrachloromethane
30 h; Heating;
参考文献
Haynes, Richard K.; Vonwiller, Simone C.; Stokes, John P.; Merlino, Louisa M.
Australian Journal of Chemistry, 1988 , vol. 41, # 6 p. 881 - 895
反应条件
Yield given. Multistep reaction;
参考文献
Craig, Donald; Ley, Steven V.; Simpkins, Nigel S.; Whitham, Gordon H.; Prior, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1949 - 1952
反应条件
hydrogenchloride in ethanol
0.5 h; Heating;
参考文献
Chimichi; Cosimelli; Bruni; Selleri
Canadian Journal of Chemistry, 1992 , vol. 70, # 4 p. 1093 - 1097
反应条件
hydrogenchloride in ethanol
0.5 h; Heating;
参考文献
Chimichi; Cosimelli; Bruni; Selleri
Canadian Journal of Chemistry, 1992 , vol. 70, # 4 p. 1093 - 1097
反应条件
in ethanol
0.5 h; Heating; Yield given;
参考文献
Chimichi; Cosimelli; Bruni; Selleri
Canadian Journal of Chemistry, 1992 , vol. 70, # 4 p. 1093 - 1097
反应条件
1: in toluene
Reflux;
2: With water; sodium hydroxide in methanol
Reflux;
3: With hydrogenchloride in methanol; water
pH=7;
参考文献
Arora, Nidhi; Chen, Shaoqing; Hermann, Johannes Cornelius; Kuglstatter, Adreas; Labadie, Sharada Shenvi; Lin, Clara Jeou Jen; Lucas, Matthew C.; Moore, Amy Geraldine; Papp, Eva; Talamas, Francisco Xavier; Wanner, Jutta; Zhai, Yansheng
Patent: US2012/15962 A1, 2012 ;
Location in patent: Page/Page column 67 ;
US 20120015962 A1
反应条件
1: NaH / bis-(2-methoxy-ethyl) ether
2: LiAlH4
View Scheme
参考文献
Vig,O.P. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1976 , vol. 14B, p. 926 - 928