4,4-二甲氧基-2-丁酮合成路线 （共 125 条）
反应条件
sodium methylate in methanol T=45 - 50°C; 6 h;
参考文献
Burdeska, Kurt; Fuhrer, Hermann; Kabas, Guglielmo; Siegrist, Adolf Emil
Helvetica Chimica Acta, 1981 , vol. 64, # 1 p. 113 - 152
参考文献
Franke; Kraft
Angewandte Chemie, 1955 , vol. 67, p. 395,398
参考文献
Burness
Journal of Organic Chemistry, 1956 , vol. 21, p. 102
Org. Synth. Coll. Vol., 1963 , vol. IV, p. 628
反应条件
hydrazine hydrate; acetic acid T=85°C; 1.5 h;
参考文献
Heterocycles, , vol. 71, # 9 p. 1967 - 1974
参考文献
Yamada
Yakugaku Zasshi, 1951 , vol. 71, p. 1349,1354
Chem.Abstr., 1952 , p. 8033
Full Text Show Details
Hata et al.
Yakugaku Zasshi, 1949 , vol. 69, p. 477
Chem.Abstr., 1950 , p. 3455
Full Text Show Details
Farbenfabr.Bayer
Patent: DE871303 , 1951 ;
反应条件
phosphoric acid Reflux;
参考文献
Duan, Yu Lian; Shi, Yong Gang; Wu, Xiang Hua; Zhang, Jun Feng; Wang, Guang Ke; Zhou, Ying; Chen, Jian Hua
Tetrahedron Letters, 2012 , vol. 53, # 48 p. 6544 - 6547,4
反应条件
hydrogenchloride in dichloromethane 2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Berkaoui, M'hamed; Outurquin, Francis; Paulmier, Claude
Tetrahedron, 1998 , vol. 54, # 31 p. 9055 - 9066
反应条件
sulfuric acid in methanol; toluene 10 h; Heating;
参考文献
Reimann; Poschl
Pharmazie, 1995 , vol. 50, # 9 p. 589 - 592
参考文献
Allen et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 787,792
参考文献
Allen et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 787,792
