N-苄基-4-甲基苯甲酰胺合成路线 (共 58 条)
反应条件
1,4-diaza-bicyclo[2.2.2]octane; bicycloheptadienemolybdenunim tetracarbonyl; tetrabutylammomium bromide in diethylene glycol dimethyl ether
T=140°C; 1.5 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Motevalli, Somayeh; Talebi, Mohsen
Tetrahedron, 2013 , vol. 69, # 1 p. 418 - 426
反应条件
oxygen; sodium hydroxide in tetrahydrofuran; water
T=25°C; 12 h;
参考文献
Soule, Jean-Francois; Miyamura, Hiroyuki; Kobayashi, Shu
Chemistry - An Asian Journal, 2013 , vol. 8, # 11 p. 2614 - 2626
反应条件
potassium carbonate in toluene
T=105°C; P=3000.3 Torr; 12 h;
参考文献
Dang, Tuan T.; Zhu, Yinghuai; Ngiam, Joyce S. Y.; Ghosh, Subhash C.; Chen, Anqi; Seayad, Abdul M.
ACS Catalysis, 2013 , vol. 3, # 6 p. 1406 - 1410
反应条件
tert.-butylhydroperoxide; manganese(IV) oxide in water; acetonitrile
T=80°C; 48 h;
参考文献
Vanjari, Rajeshwer; Guntreddi, Tirumaleswararao; Singh, Krishna Nand
Organic Letters, 2013 , vol. 15, # 18 p. 4908 - 4911
反应条件
boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid in chloroform
T=20°C; 5 h;
参考文献
An, Gwang-Il; Rhee, Hakjune
Synlett, 2003 , # 6 p. 876 - 878
反应条件
1H-imidazole; 1,1'-bis-(diphenylphosphino)ferrocene; potassium tert-butylate; palladium diacetate
T=190°C; Heck carbonylation; 0.25 h; microwave;
参考文献
Wan, Yiqian; Alterman, Mathias; Larhed, Mats; Hallberg, Anders
Journal of Organic Chemistry, 2002 , vol. 67, # 17 p. 6232 - 6235
反应条件
dicobalt octacarbonyl in benzene
T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave; Further byproducts given;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
反应条件
sodium carbonate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in water
T=170°C; 0.166667 h; microwave irradiation;
参考文献
Wu, Xiongyu; Larhed, Mats
Organic Letters, 2005 , vol. 7, # 15 p. 3327 - 3329
反应条件
4-(N,N-dimethlyamino)pyridine; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane
T=160°C; 0.333333 h; Microwave irradiation;
参考文献
Odell, Luke R.; Saevmarker, Jonas; Larhed, Mats
Tetrahedron Letters, 2008 , vol. 49, # 42 p. 6115 - 6118
反应条件
trifluoroacetic acid in acetonitrile
T=92°C; 0.166667 h; Inert atmosphereUV-irradiation;
参考文献
Zhang, Yuan; Blackman, Melissa L.; Leduc, Andrew B.; Jamison, Timothy F.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 15 p. 4251 - 4255
Angew. Chem., 2013 , vol. 125, # 15 p. 4345 - 4349,5