(7Z,9e)-7,9-乙酸十二二烯酯合成路线 （共 87 条）
反应条件
Amberlite resin
Yield given. Multistep reaction;
参考文献
Ratovelomanana, Victorin; Linstrumelle, Gerard
Tetrahedron Letters, 1981 , vol. 22, p. 315 - 318
反应条件
acetic acid
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cassani, G.; Massardo, P.; Piccardi, P.
Tetrahedron Letters, 1980 , vol. 21, p. 3497 - 3498
参考文献
Diego, Dennis G.; Cunha, Rodrigo L.O.R.; Comasseto, Joao V.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7147 - 7148
反应条件
1: 98 percent / perchloric acid / 3 h
2: 1.) (Ph3P)4Pd, 2.) copper iodide / 1.) C6H6, 40 min, 2.) 48 h, room temperature
3: diisoamylborane / 89 h
View Scheme
参考文献
Descoins, C.; Lettere, M.; Linsrumelle, G.; Michelot, D.; Ratovelomanana, V.
Synthetic Communications, 1984 , vol. 14, # 8 p. 761 - 774
反应条件
1: 1.) (Ph3P)4Pd, 2.) copper iodide / 1.) C6H6, 40 min, 2.) 48 h, room temperature
2: diisoamylborane / 89 h
View Scheme
参考文献
Descoins, C.; Lettere, M.; Linsrumelle, G.; Michelot, D.; Ratovelomanana, V.
Synthetic Communications, 1984 , vol. 14, # 8 p. 761 - 774
反应条件
in pyridine
Yield given;
参考文献
Dressaire; Langlois
Tetrahedron Letters, 1980 , vol. 21, # 1 p. 67 - 70
反应条件
2: 1) Na/Hg, 2) pyridine, HOAc / 1) MeOH, EtOAc, -35 deg C, 5 h, 2) 0 deg C, overnight
View Scheme
参考文献
Kulkarni, S. M.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1208 - 1210
反应条件
1: (i) Li2CuCl4, (ii) TsOH, aq. MeOH
2: pyridine / Ambient temperature
View Scheme
参考文献
Descoins,C. et al.
Bulletin de la Societe Chimique de France, 1977 , p. 941 - 946
反应条件
pyridine; sodium amalgam; acetic acid
1) MeOH, EtOAc, -35 deg C, 5 h, 2) 0 deg C, overnight; Yield given. Multistep reaction;
参考文献
Kulkarni, S. M.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1208 - 1210
参考文献
Labovitz,J.N. et al.
Tetrahedron Letters, 1975 , p. 4209 - 4212
