2,6-二甲基-1-苯并呋喃-3(2H)-酮合成路线 (共 4 条)
反应条件
aluminium trichloride in benzene
T=0°C; 2 h;
参考文献
Kesavulu Reddy; Krishna Rao
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 372 - 375
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=170°C; 1.5 h; Microwave irradiation;
参考文献
Farran, Daniel; Bertrand, Philippe
Synthetic Communications, 2012 , vol. 42, # 7 p. 989 - 1001
反应条件
1: 93 percent / anhyd. K2CO3 / acetone / 20 h / Heating
2: 93 percent / KOH / H2O; ethanol / 3 h / Heating
4: 82 percent / AlCl3 / benzene / 2 h / 0 °C
View Scheme
参考文献
Kesavulu Reddy; Krishna Rao
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 372 - 375
反应条件
in diethyl ether
2.) reflux, 1 h;
参考文献
Kesavulu Reddy; Krishna Rao
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 372 - 375