3-甲基-2-硝基苯甲酸合成路线 （共 57 条）
参考文献
Wheeler; Hoffman
American Chemical Journal, 1910 , vol. 44, p. 122,508
American Chemical Journal, 1911 , vol. 45, p. 445
反应条件
thionyl chloride T=0 - 20°C; 10 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Tetrahedron, , vol. 69, # 32 p. 6679 - 6686
反应条件
sodium hydroxide; thionyl chloride in methanol; water
反应条件
in hexane; acetone 3 h;
参考文献
US2005/222141 A1, ;
Page/Page column 30 ;
参考文献
Journal of the Chemical Society, , p. 2067,2070
反应条件
1: permanganate 2: tin (II)-chloride; glacial acetic acid; hydrochloric acid View Scheme
参考文献
James; Kenner; Stubbings
Journal of the Chemical Society, 1920 , vol. 117, p. 775
参考文献
Ciba-Geigy
Patent: AT341509DE2405479 , 19771974 ;
Chem.Abstr., 1974 , vol. 81, # 151817
反应条件
1.1: triethylamine; isopropyloxycarbonylchloride / dichloromethane / 1 h / 0 °C 1.2: 0.5 h / 0 °C 2.1: trifluoroacetic anhydride / dichloromethane / 1 h / 0 °C View Scheme
参考文献
PFIZER INC.; DOUNAY, Amy Beth; HELAL, Christopher John; TUTTLE, Jamison Bryce; VERHOEST, Patrick Robert
Patent: WO2012/73146 A1, 2012 ;
WO 2012/073146 A1
反应条件
1: zinc dust; alkaline alcohol 2: 200 °C View Scheme
参考文献
Freundler
Bulletin de la Societe Chimique de France, 1907 , vol. <4> 1, p. 216
Bulletin de la Societe Chimique de France, 1911 , vol. <4> 9, p. 602,657
