3-甲基-2-硝基苯甲酸合成路线 （共 57 条）
参考文献
Wheeler; Hoffman
American Chemical Journal, 1910 , vol. 44, p. 122,508
American Chemical Journal, 1911 , vol. 45, p. 445
反应条件
1: permanganate 2: tin (II)-chloride; glacial acetic acid; hydrochloric acid 3: Diazotization.man erhitzt die Diazoniumsalz-Loesung mit Jod-Kaliumjodid-Loesung auf 80grad View Scheme
参考文献
James; Kenner; Stubbings
Journal of the Chemical Society, 1920 , vol. 117, p. 775
反应条件
1: SF4 2: H2 / Raney-Ni / methanol View Scheme
参考文献
Ciba-Geigy
Patent: AT341509DE2405479 , 19771974 ;
Chem.Abstr., 1974 , vol. 81, # 151817
反应条件
1.1: EtOCOCl; Et3N / tetrahydrofuran / 10 °C 1.2: tetrahydrofuran 2.1: H2 / Pd/C / ethanol View Scheme
参考文献
Lahm, George P.; Selby, Thomas P.; Freudenberger, John H.; Stevenson, Thomas M.; Myers, Brian J.; Seburyamo, Gilles; Smith, Ben K.; Flexner, Lindsey; Clark, Christopher E.; Cordova, Daniel
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 22 p. 4898 - 4906
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=80°C; 3 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 4 p. 824 - 827
反应条件
1: tin; hydrochloric acid 2: diluted sulfuric acid; potassium nitrite View Scheme
参考文献
Findeklee
Chemische Berichte, 1905 , vol. 38, p. 3555
反应条件
copper(I) oxide T=120°C; 24 h; Ionic liquid;
参考文献
Kessler, Michael T.; Gedig, Christian; Sahler, Sebastian; Wand, Patricia; Robke, Silas; Prechtl, Martin H. G.
Catalysis Science and Technology, 2013 , vol. 3, # 4 p. 992 - 1001
反应条件
1: HCl / 6 h / 80 °C 2: dimethylformamide / 6.5 h / 100 °C 3: H2 / 5percent Pd/C View Scheme
参考文献
Kamiya; Matsui; Shirahase; Nakamura; Wada; Kanda; Shimaji; Kakeya
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 10 p. 1692 - 1695
反应条件
sodium azide; sulfuric acid
参考文献
Courtin,A.
Helvetica Chimica Acta, 1976 , vol. 59, p. 379 - 387
反应条件
1: 89 percent / H2SO4 / 24 h / Heating 2: 49 percent / N-bromosuccinimide; benzoyl peroxide / CCl4 / Heating View Scheme
参考文献
Fader, Lee D.; Myers, Eddie L.; Tsantrizos, Youla S.
Tetrahedron, 2004 , vol. 60, # 10 p. 2235 - 2246
