1,4-二苯基-3,3-二甲基氮杂环丁烷-2-酮合成路线 （共 28 条）
反应条件
1: 86 percent / AlCl3, LiAlH4 / diethyl ether / 4 h / Heating 2: 500 °C / 0 Torr View Scheme
参考文献
Lesniak, S.
Polish Journal of Chemistry, 1995 , vol. 69, # 11 p. 1484 - 1489
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether 4 h; Heating;
参考文献
Lesniak, S.
Polish Journal of Chemistry, 1995 , vol. 69, # 11 p. 1484 - 1489
反应条件
T=680°C; P=0.002 Torr; Yields of byproduct given;
参考文献
Bartnik, R.; Lesniak, S.
Polish Journal of Chemistry, 1994 , vol. 68, # 12 p. 2605 - 2612
反应条件
T=680°C; P=0.002 Torr; Yields of byproduct given;
参考文献
Bartnik, R.; Lesniak, S.
Polish Journal of Chemistry, 1994 , vol. 68, # 12 p. 2605 - 2612
反应条件
1: 86 percent / AlCl3, LiAlH4 / diethyl ether / 4 h / Heating 2: 500 °C / 0 Torr View Scheme
参考文献
Lesniak, S.
Polish Journal of Chemistry, 1995 , vol. 69, # 11 p. 1484 - 1489
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane
1 h; Inert atmosphereCooling;
2: With water in tetrahydrofuran; hexane
1 h; Inert atmosphereCooling;
参考文献
Geherty, Maryll; Melnyk, James; Chomsky, Keith; Hunt, David A.
Tetrahedron Letters, 2013 , vol. 54, # 36 p. 4934 - 4936
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane
1 h; Inert atmosphereCooling;
2: With water in tetrahydrofuran; hexane
1 h; Inert atmosphere;
参考文献
Geherty, Maryll; Melnyk, James; Chomsky, Keith; Hunt, David A.
Tetrahedron Letters, 2013 , vol. 54, # 36 p. 4934 - 4936
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane
1 h; Inert atmosphereCooling;
2: With water in tetrahydrofuran; hexane
1 h; Inert atmosphere;
参考文献
Geherty, Maryll; Melnyk, James; Chomsky, Keith; Hunt, David A.
Tetrahedron Letters, 2013 , vol. 54, # 36 p. 4934 - 4936
反应条件
triphenyl phosphite; Et2(Me)SiH; [RhCl(η2:η2-cycloocta-1,5-diene)]2
T=60°C; Mannich addition-cyclization; 6 h;
参考文献
Townes, Jennifer A.; Evans, Michael A.; Queffelec, Jerome; Taylor, Steven J.; Morken, James P.
Organic Letters, 2002 , vol. 4, # 15 p. 2537 - 2540
反应条件
iodine; zinc in 1,4-dioxane
T=20°C; Reformatsky reaction; 0.0833333 h; sonication;
参考文献
Ross, Nathan A.; MacGregor, Robert R.; Bartsch, Richard A.
Tetrahedron, 2004 , vol. 60, # 9 p. 2035 - 2041
