3,4,5-三氯吡啶-2-甲酸合成路线 （共 14 条）
反应条件
1,4-dihydroquinoline; palladium diacetate; 1,3-bis-(diphenylphosphino)propane in water; triethylamine T=80°C; P=20251.6 Torr; 3 h;
参考文献
Heterocycles, , vol. 63, # 2 p. 411 - 417
反应条件
1: With palladium diacetate; 1,3-bis-(diphenylphosphino)propane; sodium carbonate in various solvent(s) T=120 - 130°C; 2: With lithium hydroxide; water T=90°C; 1 h;
参考文献
Hull Jr., John W.; Wang, Chen
Heterocycles, 2004 , vol. 63, # 2 p. 411 - 417
反应条件
sulfuric acid T=120 - 130°C;
参考文献
Journal of the Chemical Society, , vol. 87, p. 801
Journal of the Chemical Society, , vol. 93, p. 1993
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 148, p. 13,16
反应条件
1: hydrogen chloride; chlorine / 105 - 110 °C 2: sulfuric acid / 120 - 130 °C View Scheme
参考文献
Journal of the Chemical Society, , vol. 87, p. 801
Journal of the Chemical Society, , vol. 93, p. 1993
反应条件
1: POCl3; PCl5 3: ethanolic alkaline solution View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 148, p. 13,16
参考文献
Sell
Journal of the Chemical Society, 1905 , vol. 87, p. 801
Journal of the Chemical Society, 1908 , vol. 93, p. 1993
反应条件
1: hydrogen chloride 2: aqueous methanol; ammonia View Scheme
参考文献
Sell
Journal of the Chemical Society, 1905 , vol. 87, p. 801
Journal of the Chemical Society, 1908 , vol. 93, p. 1993
反应条件
phosphorus; hydrogen iodide
参考文献
Graf
Journal fuer Praktische Chemie (Leipzig), 1937 , vol. <2> 148, p. 13,16
反应条件
phosphorus; hydrogen iodide
参考文献
Graf
Journal fuer Praktische Chemie (Leipzig), 1937 , vol. <2> 148, p. 13,16
