in neat (no solvent) (exclusion of moisture); room temp., 16 h; purifn. by trap-to-trap distn.;
参考文献
Aldridge, Simon; Blake, Alexander J.; Downs, Anthony J.; Parsons, Simon; Pulham, Colin R.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 6 p. 853 - 859