tricarbonyl(η6-arene)chromium(0) complex derived from (1S,2R)-N,N-dibutylnorephedrine in hexane; toluene T=0°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
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Sprout, Christopher M.; Seto, Christopher T.
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7788 - 7794
1: With N,N-bis(3,5-di-t-butylbenzyl)-O-benzyl-L-α-aspartyl-L-proline methyl ester in toluene T=0 - 20°C; 48 h; Inert atmosphere; 2: With hydrogenchloride in water; toluene Inert atmosphere; optical yield given as percent eeenantioselective reaction;
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Kang, Seock Yong; Park, Yong Sun
European Journal of Organic Chemistry, 2012 , # 9 p. 1703 - 1706
in diethyl ether Si2Cl6 and 31percent excess of Zn(CH3)2 in ether at 85°C in a closed tube;;
参考文献
Brockway, L. O.; Davidson, N. R.
Journal of the American Chemical Society, 1941 , vol. 63, p. 3287 - 3297
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Gmelin Handbook: Si: MVol.C, 113, page 316 - 320
