6-苄基氨基-9-甲基嘌呤合成路线 （共 6 条）
反应条件
Raney Ni W-2 in ethanol
T=50°C; 8 h;
参考文献
Fujii; Saito; Sakuma; Minami; Inoue
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 3 p. 652 - 660
反应条件
in water
12 h; Heating;
参考文献
Gasque, C. Edward
Phytochemistry (Elsevier), 1982 , vol. 21, # 7 p. 1501 - 1508
反应条件
sodium hydroxide in ethanol
T=-5°C; 3 h; Reflux;
参考文献
Krueger, Thomas; Wagner, Christoph; Bruhn, Clemens; Lis, Tadeusz; Steinborn, Dirk
Journal of Molecular Structure, 2008 , vol. 891, # 1-3 p. 110 - 114
反应条件
1: 12 percent / AcNMe2 / 30 h / 30 °C
2: 71 percent / Raney Ni W-2 / ethanol / 8 h / 50 °C
View Scheme
参考文献
Fujii; Saito; Sakuma; Minami; Inoue
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 3 p. 652 - 660
反应条件
1: 12 percent / AcNMe2 / 30 h / 30 °C
2: 71 percent / Raney Ni W-2 / ethanol / 8 h / 50 °C
View Scheme
参考文献
Fujii; Saito; Sakuma; Minami; Inoue
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 3 p. 652 - 660
反应条件
tetra(n-butyl)ammonium hydroxide; triethylamine
1.) CH2Cl2, RT, 6 h, 2.) n-butanol, reflux, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Havlicek, Libor; Hanus, Jan; Vesely, Jaroslav; Leclerc, Sophie; Meijer, Laurent; Shaw, Gordon; Strnad, Miroslav
Journal of Medicinal Chemistry, 1997 , vol. 40, # 4 p. 408 - 412
