1: 73 percent / tetrafluoroboric acid, sodium nitrite / H2O / 0.5 h / -10 °C
2: 98 percent / tetrathiafulvalene / acetone / 2 °C
View Scheme
参考文献
Murphy, John A.; Roome, Stephen J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1349 - 1358
1: 70.5 percent / copper acetylacetonate, NaBH4 / ethanol / 2 h / Ambient temperature
2: 73 percent / tetrafluoroboric acid, sodium nitrite / H2O / 0.5 h / -10 °C
3: 98 percent / tetrathiafulvalene / acetone / 2 °C
View Scheme
参考文献
Murphy, John A.; Roome, Stephen J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1349 - 1358
1: 78.2 percent / tetrahydrofuran / 0.5 h
2: 70.5 percent / copper acetylacetonate, NaBH4 / ethanol / 2 h / Ambient temperature
3: 73 percent / tetrafluoroboric acid, sodium nitrite / H2O / 0.5 h / -10 °C
4: 98 percent / tetrathiafulvalene / acetone / 2 °C
View Scheme
参考文献
Murphy, John A.; Roome, Stephen J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1349 - 1358