3-苯基异恶唑-5-基甲胺合成路线 （共 9 条）
反应条件
1: With methanesulfonyl chloride; triethylamine in dichloromethane T=20°C; 6 h; Cooling; 2: With sodium azide in N,N-dimethyl-formamide T=55°C; 8 h; 3: With ammonium chloride; zinc in ethanol; water 0.5 h; Reflux;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 50, # 5 p. 695 - 703
反应条件
1: 45 percent / NaOCl, TEA / CH2Cl2; H2O / 0 °C 2: 85 percent / TFA / CH2Cl2 View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 47 p. 7509 - 7512
反应条件
1: hydroxylamine hydrochloride 2: sodium hypochlorite; triethylamine / dichloromethane; water / 0 - 20 °C 3: N,N-dimethyl-formamide / 5 h / 20 °C 4: hydrazine hydrate / ethanol / 5 h / Reflux View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 58, # 5 p. 2685 - 2689
反应条件
in benzene 48 h; Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, # 6 p. 1597 - 1598
反应条件
1: triethylamine / benzene / 0.17 h 2: 15 percent / benzene / 48 h / Ambient temperature View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, # 6 p. 1597 - 1598
反应条件
1: N,N-dimethyl-formamide / 5 h / 20 °C 2: hydrazine hydrate / ethanol / 5 h / Reflux View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 58, # 5 p. 2685 - 2689
反应条件
hydrazine hydrate in ethanol Gabriel reaction; 5 h; Reflux;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 58, # 5 p. 2685 - 2689
反应条件
ammonium chloride; zinc
参考文献
Archives of Pharmacal Research, , vol. 33, # 6 p. 831 - 842
