N-甲基-1-(2-硝基苯基)甲胺合成路线 （共 4 条）
反应条件
sodium cyanoborohydride in methanol
T=110°C; 0.183333 h; Microwave irradiation;
参考文献
Bruno, Claudio; Lentini, Giovanni; Catalano, Alessia; Carocci, Alessia; Lovece, Angelo; Di Mola, Antonia; Cavalluzzi, Maria Maddalena; Tortorella, Paolo; Loiodice, Fulvio; Iaccarino, Guido; Campiglia, Pietro; Novellino, Ettore; Franchini, Carlo
Synthesis, 2010 , # 24 art. no. T14310SS, p. 4193 - 4198
反应条件
in methanol; water
0.75 h; Heating;
参考文献
Golec, Frederick A.; Reilly, Laurence W.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 789 - 790
反应条件
1: 15.35 g / H2O / 0.25 h
2: 1.) NaBH4, 2.) hydrochloric acid / 1.) ethanol, room temp., 4 h., 2.) ether
View Scheme
参考文献
Zara-Kaczian, Erzsebet; Deak, Gyula; Gyoergy, Lajos
Acta Chimica Hungarica, 1989 , vol. 126, # 4 p. 441 - 454
反应条件
hydrogenchloride; sodium tetrahydroborate
1.) ethanol, room temp., 4 h., 2.) ether; Yield given. Multistep reaction;
参考文献
Zara-Kaczian, Erzsebet; Deak, Gyula; Gyoergy, Lajos
Acta Chimica Hungarica, 1989 , vol. 126, # 4 p. 441 - 454
