1,5-双-(甲基硫代)-戊烷合成路线 (共 9 条)
参考文献
The University of Wales Swansea
Patent: EP866049 A2, 1998 ;
反应条件
1: poly(pentamethylenedisulfide) With sodium hydroxide; hydrazine hydrate in water
T=75°C; 2 h;
2: methyl iodide in water
T=40°C;
参考文献
Alekminskaya; Russavskaya; Korchevin; Deryagina; Trofimov
Russian Journal of General Chemistry, 2000 , vol. 70, # 5 p. 732 - 737
反应条件
18-crown-6 ether; potassium carbonate
T=100°C; 8 h;
参考文献
Lissel, Manfred; Schmidt, Stefan; Neumann, Beate
Synthesis, 1986 , # 5 p. 382 - 383
反应条件
sodium ethanolate in ethanol
12 h; Ambient temperature; Yield given;
参考文献
Anklam, Elke
Synthesis, 1987 , # 9 p. 841 - 843
反应条件
sodium ethanolate in hexane
7 h; Ambient temperature; Yield given;
参考文献
Anklam, Elke
Synthesis, 1987 , # 9 p. 841 - 843
参考文献
Protiva et al.
Chemicke Listy, 1953 , vol. 47, p. 584,587
Chem.Abstr., 1955 , p. 199
反应条件
ethanol
Behandeln des Reaktionsprodukts mit wss.Natronlauge und anschliessend mit Jodmethan.;
参考文献
Walker
Journal of the Chemical Society, 1950 , p. 193,196
参考文献
Golovnya, R. V.; Misharina, T. A.; Garbuzov, V. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, p. 1765 - 1769
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 11 p. 2503 - 2508
参考文献
Walker
Journal of the Chemical Society, 1950 , p. 193,196