N,N-二甲基-2-[2-[4-(1,1,3,3-四甲基丁基)苯氧基]乙氧基]乙胺合成路线 (共 5 条)
参考文献
Roehm and Haas Co.
Patent: US2170111 , 1936 ;
参考文献
Roehm and Haas Co.
Patent: US2229024 , 1939 ;
Full Text Show Details
Roehm and Haas Co.
Patent: US2170111 , 1936 ;
Full Text Show Details
Roehm and Haas Co.
Patent: US2115250 , 1936 ;
反应条件
1: Trriton X100 With N-benzyl-N,N,N-triethylammonium chloride in toluene
Heating / reflux;
2: 2-chloro-N,N-dimethylaminoethane in toluene
16 - 23 h; Heating / reflux;
参考文献
Dishman Pharmaceuticals and Chemicals Ltd.
Patent: EP1892235 A1, 2008 ;
Location in patent: Page/Page column 4 ;
反应条件
tetrabutylammomium bromide in water
T=130°C; 5 h; Sealed tube;
参考文献
Beijing Sunpu Biochem. Tech. Co., Ltd.; CHENG, Che Jim; SONG, Fei; PAN, Yongmei
Patent: EP2703382 A1, 2014 ;
Location in patent: Paragraph 0056; 0057; 0058 ;
反应条件
1: NaOH; water / 110 - 120 °C
2: 180 °C
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参考文献
Roehm and Haas Co.
Patent: US2229024 , 1939 ;
Full Text Show Details
Roehm and Haas Co.
Patent: US2170111 , 1936 ;
Full Text Show Details
Roehm and Haas Co.
Patent: US2115250 , 1936 ;