ammonia; tert-butyl alcohol in tetrahydrofuran
T=-78°C;
参考文献
McCague, Raymond; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2399 - 2407
ammonia; tert-butyl alcohol; methyl iodide in tetrahydrofuran
Further byproducts given;
参考文献
McCague, Raymond; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2399 - 2407
ammonia; tert-butyl alcohol in tetrahydrofuran
Further byproducts given. Title compound not separated from byproducts;
参考文献
McCague, Raymond; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2399 - 2407
ammonia; tert-butyl alcohol in tetrahydrofuran
Further byproducts given;
参考文献
McCague, Raymond; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2399 - 2407
ammonia; tert-butyl alcohol in tetrahydrofuran
Further byproducts given;
参考文献
McCague, Raymond; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2399 - 2407
Gilchrist, Thomas L.; Rees, Charles W.; Tuddenham, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3214 - 3220
lithium diisopropyl amide in tetrahydrofuran
T=-78 - 20°C;
参考文献
McCague, Raymond; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2399 - 2407
Gilchrist, Thomas L.; Rees, Charles W.; Tuddenham, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3214 - 3220
1: LiN(iPr)2 / tetrahydrofuran / -78 - 20 °C
2: H2O2 / tetrahydrofuran / -10 - 20 °C
View Scheme
参考文献
Gilchrist, Thomas L.; Rees, Charles W.; Tuddenham, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3214 - 3220
triethylamine; sodium iodide in acetonitrile
T=45°C; 2 h;
参考文献
McCague, Raymond; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2399 - 2407
