3,3-二甲基-2-异丙基丁酸甲酯合成路线 （共 7 条）
反应条件
1: 96 percent / Heating
2: 1) iPr2NLi / 1) THF, -78 deg C, 30 min, 2) -78 deg C to r.t.
3: ZnCl2 / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Lion, Claude; Dubois, Jacques-Emile
Tetrahedron, 1981 , vol. 37, p. 319 - 323
反应条件
1: 1) iPr2NLi / 1) THF, -78 deg C, 30 min, 2) -78 deg C to r.t.
2: ZnCl2 / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Lion, Claude; Dubois, Jacques-Emile
Tetrahedron, 1981 , vol. 37, p. 319 - 323
反应条件
1: 98 percent / Heating
2: 1) iPr2NLi / 1) THF, -78 deg C, 30 min, 2) -78 deg C to r.t.
3: ZnCl2 / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Lion, Claude; Dubois, Jacques-Emile
Tetrahedron, 1981 , vol. 37, p. 319 - 323
反应条件
1: 1) iPr2NLi / 1) THF, -78 deg C, 30 min, 2) -78 deg C to r.t.
2: ZnCl2 / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Lion, Claude; Dubois, Jacques-Emile
Tetrahedron, 1981 , vol. 37, p. 319 - 323
反应条件
zinc(II) chloride in dichloromethane
24 h; Ambient temperature; Yield given;
参考文献
Lion, Claude; Dubois, Jacques-Emile
Tetrahedron, 1981 , vol. 37, p. 319 - 323
反应条件
zinc(II) chloride in dichloromethane
24 h; Ambient temperature; Yield given;
参考文献
Lion, Claude; Dubois, Jacques-Emile
Tetrahedron, 1981 , vol. 37, p. 319 - 323
参考文献
Pirozhkov,S.D. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1976 , vol. 25, p. 1264 - 1267
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1976 , vol. 25, # 6 p. 1314 - 1317
