1: furan With n-butyllithium in tetrahydrofuran; hexane T=60°C; 1 h; Inert atmosphereCooling with acetone-dry ice; 2: 1,3-dibromo-propane in tetrahydrofuran; hexane T=20°C; Inert atmosphereCooling with acetone-dry ice;

暂无反应条件数据

n-butyllithium 1.) THF, hexane, 0 deg C, 1 h; room temperature, 1 h. 2.) room temperature, 15 h; Yield given. Multistep reaction;