4-(4,5-二氢-1,3-噁唑-2-基)苯胺合成路线 （共 4 条）
反应条件
5 palladium over charcoal in ethanol; ethyl acetate
T=20°C; 72 h;
参考文献
DAIICHI PHARMACEUTICAL CO., LTD.
Patent: EP1612204 A1, 2006 ;
Location in patent: Page/Page column 37 ;
反应条件
1: zinc(II) chloride
2: palladium 10 on activated carbon; ammonium formate / ethanol / Reflux
View Scheme
参考文献
Gordey, Erin E.; Yadav, Paras N.; Merrin, Marcus P.; Davies, Jill; Ward, Steven A.; Woodman, Grant M.J.; Sadowy, Amber L.; Smith, Todd G.; Gossage, Robert A.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 15 p. 4512 - 4515
反应条件
sodium hydrogencarbonate; N,N',N''-tris(1H-1,2,4-triazole)phosphoric triamide
1.) acetonitrile, pyridine, room temp., 3 min., 2.) 10 min.; Yield given. Multistep reaction;
参考文献
Sund, Christian; Ylikoski, Jyrki; Kwiatkowski, Marek
Synthesis, 1987 , # 9 p. 853 - 854
反应条件
[{Cu(MeOH)}4(µ-5(3)-(methoxycarbonyl)-pyrazole-3(5)-carboxylato)4]·4MeOH·0.5H2O
T=100°C; 6 h; Catalytic behavior; Reagent/catalyst;
参考文献
Wang, Ling; Guo, Bin; Li, Hong-Xi; Li, Qi; Li, Hai-Yan; Lang, Jian-Ping
Dalton Transactions, 2013 , vol. 42, # 44 p. 15570 - 15580
