(4-甲氧基-2,3,6-三甲基苄基)-三苯基鏻溴化物合成路线 （共 4 条）
反应条件
hydrogenchloride in methanol; water
96 h; Ambient temperature;
参考文献
Bestmann; Ermann
1984 , vol. 1984, # 10 p. 1740 - 1745
反应条件
1: 1.) POCl3 / 1.) 0 deg C, 2 h, 2.) 70 deg, 24 h
2: 93 percent / LiAlH4
3: 95 percent / 38 percent HCl / methanol; H2O / 96 h / Ambient temperature
View Scheme
参考文献
Bestmann; Ermann
1984 , vol. 1984, # 10 p. 1740 - 1745
反应条件
1: 61 percent / KOH / 0.5 h / Heating
2: 1.) POCl3 / 1.) 0 deg C, 2 h, 2.) 70 deg, 24 h
3: 93 percent / LiAlH4
4: 95 percent / 38 percent HCl / methanol; H2O / 96 h / Ambient temperature
View Scheme
参考文献
Bestmann; Ermann
1984 , vol. 1984, # 10 p. 1740 - 1745
反应条件
1: 93 percent / LiAlH4
2: 95 percent / 38 percent HCl / methanol; H2O / 96 h / Ambient temperature
View Scheme
参考文献
Bestmann; Ermann
1984 , vol. 1984, # 10 p. 1740 - 1745
