delta-2,2'-联[1,3-二硒杂环戊烯]合成路线 （共 5 条）
反应条件
morpholine; iodine in N,N-dimethyl-formamide
T=20°C; 2 h;
参考文献
Takimiya, Kazuo; Jeon, Hyung Joon; Otsubo, Tetsuo
Synthesis, 2005 , # 16 art. no. F10005SS, p. 2810 - 2813
反应条件
1: With selenium in tetrahydrofuran; xylene
T=-70 - 0°C;
2: in methanol
T=-78 - 0°C;
参考文献
Takimiya, Kazuo; Jeon, Hyung Joon; Otsubo, Tetsuo
Synthesis, 2005 , # 16 art. no. F10005SS, p. 2810 - 2813
反应条件
phosphorous acid trimethyl ester in benzene
1.5 h; Heating;
参考文献
Takimiya, Kazuo; Kataoka, Yoshiro; Niihara, Naoto; Aso, Yoshio; Otsubo, Tetsuo
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5217 - 5224
反应条件
1: in toluene
1 h; Heating;
2: With phosphorous acid trimethyl ester in toluene
3 h; Heating;
参考文献
Kodani; Takimiya; Aso; Otsubo; Nakayashiki; Misaki
Synthesis, 2001 , # 11 p. 1614 - 1618
反应条件
phosphorous acid trimethyl ester in benzene
2 h; Heating; Yield given;
参考文献
Johannsen, Ib; Lerstrup, Knud; Henriksen, Lars; Bechgaard, Klaus
Journal of the Chemical Society, Chemical Communications, 1984 , # 2 p. 89 - 90
