1: benzene / 40 h / Heating 2: CrO3, acetic acid / 1 h / Heating View Scheme

sodium chlorite; citrate-phosphate buffer in water T=-5°C; 0.333333 h;

sodium hydroxide; dihydrogen peroxide und anschliessend mit FeCl3 in wss.HCl;

ethanol

sodium dichromate

暂无反应条件数据

1: CsF/celite, 18-crown-6-ether / dimethylformamide / Heating 2: 1.) cetyltrimethylammonium bromide, aq. Na2S2O4, 2.) aq. KOH / 1.) THF, 2.) THF, RT, 14 h 3: 88 percent / 2N aq. KOH / 24 h / Ambient temperature 4: 1.) POCl3, 2.) 1N aq. HCl / 1.) reflux, 1 h, 2.) reflux, 1 h 5: 76 percent / K2CO3 / acetone View Scheme

Yield given. Multistep reaction;