Zimin, M. G.; Zabirov, N. G.; Smirnov, V. N.; Cherkasov, R. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 1 p. 24 - 30,18 - 23
Crank, George; Mursyidi, Achmad
Australian Journal of Chemistry, 1982 , vol. 35, # 4 p. 775 - 784
→
反应条件
in dichloromethane
Irradiation (UV/VIS); addn. of soln. of radical precursor to soln. of Co-compd. in CH2Cl2 at 0°C (under N2) with stirring, illumination with a 500 W sunlamp for 12 h; bringing to room temp., concn. the volume, chromy. (silica gel, eluent: pentane and CH2Cl2 for organic products, CH2Cl2/ethyl acetate for inorganic product), elem. anal.;
参考文献
Das, Indira; Roy, Sujit
Journal of Organometallic Chemistry, 1994 , vol. 464, # 2 p. 233 - 238
1: 4-dimethylamino-benzaldehyde in dimethyl sulfoxide
2: trichloroacetonitrile With triethylamine; copper(l) chloride in water; dimethyl sulfoxide
T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Nenajdenko; Shastin; Golubinskii; Lenkova; Balenkova
Russian Chemical Bulletin, 2004 , vol. 53, # 1 p. 228 - 232
1: trichloroacetonitrile With triphenylphosphine in acetonitrile
1 h; Heating;
2: benzaldehyde in acetonitrile
6 h; Heating; Title compound not separated from byproducts;
参考文献
Matveeva; Erin; Osetrov; Leshcheva; Kurts
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 3 p. 388 - 392
Zimin, M. G.; Zabirov, N. G.; Smirnov, V. N.; Cherkasov, R. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 1 p. 24 - 30,18 - 23
